Abstract
Di-t-butyl nitroxide readily substitutes alkyl zirconocenes and hafnocenes, Cp 2MR 2, by a rate-determining displacement of alkyl radicals to give high yields of O-alkyl- N, N-di-t-butylhydroxylamine and Cp 2M(R)ONBu t 2. A free radical substitution of di-benzylzirconocene by benzenethiyl radicals yields Cp 2Zr(SPh) 2.
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