Abstract
Distinctive features of an experimental procedure for determination of the conversion of sodium borohydride in hydrolysis in an aqueous-alkaline medium are described; the procedure is based on measuring the amount of the released hydrogen. Technical and methodological features of implementation of this procedure and measurement errors are discussed; a technique for calculation of the conversion of sodium borohydride in hydrolysis is presented. Experimental data in the form of the constants of a quasistationary hydrolysis regime are given for different isothermal conditions. The range of experiments covers temperatures from 20 to 95°C and alkali concentrations from 10−2 to 5 M.
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