Abstract

A recently developed 14-kW 240 ° electron beam gun was installed in an 18-in. glass belljar pumped by a liquid-helium cryopumping system made by Air Liquide, a French supplier of cryogenic pumps. The cryogenic pump has a speed of 6000 liter/sec for air. Pumping of hydrogen and helium is accomplished by bleeding in a small amount of argon which freezes on the helium reservoir and has a gettering effect on these gases. Experiments were conducted to determine the operating characteristics of this type of system when evaporating various materials such as aluminum, copper, and tantalum. Data taken during the evaporation runs consisted of major gases evolved, time for belljar pressure to recover to 10−7 Torr range, pressure during evaporation, effectiveness of argon sublimator in reducing pressure, and pumpdown curves. It was found that using a liquid-helium cryopumping system in conjunction with an electron beam gun gives exceptional results. It would be particularly advantageous in the fabrication of MOS devices where extreme cleanliness is required.

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