Effect of Desensitizing Mouth Rinses on Surface Properties of 3D-Printed Crowns: An In Vitro Study

Background: Various fluids in the oral environment can affect the surface roughness of resin composites. This in vitro study was conducted to determine the influence of the mouth rinses on surface roughness of two methacrylate-based resin (nanofilled and packable composite) and siloraine-based resin composites. Materials and methods : Disc-sh aped specimens (12 mm in diameter and 2mm in height) were prepared from three types of composite resin materials: Filtek™ Z350 XT, Filtek™ P60 and Filtek™ P90.Thirty specimens were prepared from each composite type and subdivided into three subgroups (n=10 ) according to the type of treatment solution: distilled water (control), Listerine (alcohol-containing), Sensodyne Pronamel (alcohol free fluoride- containing). Each subgroup was immersed in 20 ml of treatment solutions and incubated at 37°C for 24 hr and then subjected to surface roughness test by profilometer .The resulting data were statistically analyzed using ANOVA and LSD test at0.05 significance level. Results : The results of this study showed that both mouth rinses irrespective of the presence or absence of alcohol resulted in significant increase in the surface roughness of the tested resin composite materials compared to control with no significant difference between the two mouth rinses. Comparison among the three types of resin in each treatment solution showed that there was a statistically high significant difference in surface roughness between all subgroups Conclusion : Both alcohol-containing and alcohol-free fluoride containing mouth rinses cause highly significant increase in surface roughness of composite resins. Composite changes depended on the material itself rather than the mouth rinse solution used. Key word s : Composite resin, mouth rinses, siloraine, surfaces roughness.

Assessment of enamel surface roughness and hardness with metal and ceramic orthodontic brackets using different etching and adhesive systems: An in vitro study

BackgroundTo evaluate the impacts of various charcoal-containing whitening toothpastes on color stability and surface roughness of a supra-nanofilled composite resin.MethodsA total of 105 disc-shaped specimens were fabricated using a supra-nano spherical-filled composite resin and immersed in a coffee solution to induce staining. Color and surface roughness were measured before (T0) and after staining process (T1). The specimens were randomly allocated into seven groups (n = 15): a negative control (Distilled water, DW), a positive control (Colgate Total 12, CT12), and five groups treated with charcoal-containing whitening toothpastes: Colgate Optic White (COW), Curaprox Black Is White (CBW), R.O.C.S. Black Edition Whitening (ROCS), Ipana 3D White (IPW), and Signal Nature Elements Charcoal (SNE). Brushing was performed using an electric toothbrush three times per day for 30s over a two-week period, followed by final color and surface roughness measurements (T2). Statistical analyses were performed using one-way ANOVA, Kruskal–Wallis, Tukey’s HSD, Tamhane’s T2, and Dunn’s tests (p < 0.05).ResultsColor alterations (ΔE00) in all groups treated with charcoal-based whitening toothpastes exceeded the clinical acceptability threshold. However, no statistically significant differences in ΔE00 were noted among these groups (p > 0.05).The SNE group exhibited significantly higher ∆b values than the COW and CBW groups (p < 0.05), while the CBW group presented considerably lower ΔL values than the COW, IPW, and SNE groups (p < 0.05). A significant increase in surface roughness ​​was detected in all groups exposed to charcoal-based whitening toothpastes (p < 0.05),with statistically significant variations observed among groups (p < 0.05).ConclusionsCharcoal-containing whitening toothpastes effectively reduced coffee-induced discoloration on composite resin surface while causing a significant increase in surface roughness. The toothpastes used exhibited similar effects on color change but showed variations in surface roughness among groups.

Hybrid computer-aided design and computer-aided manufacturing (CAD/CAM) materials have gained prominence in restorative dentistry due to their advantageous mechanical and esthetic properties; however, their long-term performance may be adversely affected by acidic oral environments, such as those associated with gastroesophageal reflux disease (GERD). This in vitro study aimed to investigate the effects of simulated gastric acid exposure on the surface roughness, gloss, color stability, and microhardness of two hybrid CAD/CAM materials: Vita Enamic and Cerasmart. Standardized rectangular specimens (2 mm thickness) were prepared and polished using a clinically relevant intraoral protocol. Baseline measurements were obtained for surface roughness, gloss, color change (ΔE), and Vickers microhardness. All specimens were then immersed in hydrochloric acid (pH 1.2) for 24 h to simulate prolonged gastric acid exposure, after which the same properties were re-evaluated. Post-immersion analysis revealed significant increases in surface roughness and reductions in gloss and microhardness for both materials (p < 0.05), with Vita Enamic demonstrating greater susceptibility to degradation. Color changes remained below the clinically perceptible threshold, with no significant differences between materials. These findings highlight the potential vulnerability of hybrid CAD/CAM materials to acidic environments and underscore the importance of careful material selection in patients predisposed to acid-related challenges.

Dental restorations must replicate the natural appearance of teeth while ensuring biocompatibility and durability. This study evaluated the surface characteristics and color stability of three dental composites-Herculite Ultra XRV, G-ænial A'CHORD, and Omnichroma-exposed to acidic beverages (red wine, black coffee, and Coca-Cola). Sixty disk-shaped specimens were prepared, polished, and immersed in these beverages. Surface roughness was assessed using profilometry and SEM analysis, hydrophobicity via contact angle analysis, and surface charge through streaming potential measurements. Color stability was evaluated using a spectrophotometer, and the pH levels of the solutions were recorded. Results showed that Herculite Ultra XRV had the highest mean contact angle (79.46° ± 6.52), indicating superior hydrophobicity, while Omnichroma had the lowest (64.94° ± 3.08), indicating more hydrophilicity. Significant color changes were observed, especially in black coffee, with ∆E values indicating notable discoloration. The acidic pH of the solutions increased surface roughness and color changes. Statistical analyses confirmed significant increases in surface roughness and color change for all composites, with the nanohybrid resin composite showing the greatest variability. These findings highlight the need for dental restorative materials with enhanced resistance to acidic environments to improve the longevity and esthetics of dental treatments.

Forensic study of mechanical properties of dental fillings after immersion in marine environment

AimTo evaluate and compare the surface roughness and colour change of microhybrid and nanocomposite after exposure to beverages commonly used by children.MethodsThirty discs were prepared using Filtek Z250 and Filtek Supreme composites. Discs were immersed in distilled water, orange juice and Coca-Cola. Colour and surface roughness were measured at baseline and on days 15 and 30.ResultsFiltek Z250 and Filtek Supreme showed no significant difference in surface roughness and colour change at all measurement times. Immersion solution had a significant effect on surface roughness as well as colour change. Specimens immersed in Coca-Cola demonstrated the highest effect, followed by those immersed in orange juice, while specimens immersed in distilled water had the least effect. There was a significant increase in surface roughness and colour change over time. The change in colour was more evident in the period between baseline measurements and after 15 days. There was a significant interaction between media type and time.ConclusionsBoth composites showed no significant difference in roughness and colour change at all measurement times. There was a significant increase in surface roughness and colour change in all immersion solutions tested over time. Coca-Cola caused unacceptable colour change.

Autoclave sterilization and microwave sterilization has been suggested as the effective methods for the disinfection of elastomeric impressions, but subjecting elastomeric impressions to extreme temperature may have adverse effects on critical properties of the elastomers. To evaluate the effect of chemical disinfection as well as autoclave and microwave sterilization on the surface roughness of elastomeric impression materials. The surface roughness of five commercially available polyvinyl siloxane impression materials (Coltene President, Affinis Perfect impression, Aquasil, 3M ESPE Express and GC Exafast) were evaluated after subjecting them to chemical disinfection, autoclaving and microwave sterilization using a Talysurf Intra 50 instrument. Twenty specimens from each material were fabricated and divided into four equal groups, three experimental and one control (n=25). The differences in the mean surface roughness between the treatment groups were recorded and statistically analyzed. No statistically significant increase in the surface roughness was observed when the specimens were subjected to chemical disinfection and autoclave sterilization, increase in roughness and discoloration was observed in all the materials when specimens were subjected to microwave sterilization. Chemical disinfection did not have a significant effect but, since it is less effective, autoclave sterilization can be considered effective and autoclaving did not show any specimen discoloration as in microwave sterilization. Microwave sterilization may be considered when impressions are used to make diagnostic casts. A significant increase in surface roughness may produce rougher casts, resulting in rougher tissue surfaces for denture and cast restorations. Autoclave sterilization of vinyl polysiloxane elastomeric impressions for 5 minutes at 134°C at 20 psi may be considered an effective method over chemical disinfection and microwave sterilization, because chemical disinfection does not eliminate all disease-causing microorganisms and microwave sterilization leads to a rougher impression surface.

Aims: To evaluate the influence of post bleaching diode laser irradiation on the surface roughness of bleached enamel. Materials and methods: Forty bovine teeth were prepared and then randomly divided into two equal groups (n=20) according to the in–office bleaching technique as follows: CB: Conventional in–office bleaching technique LB: Laser–assisted in–office bleaching technique. Each group was then subdivided into two subgroups (n=10) according to laser irradiation setting as follows: C2: Conventionally bleached followed by 2-Watt laser irradiation, C4: Conventionally bleached followed by 4-Watt laser irradiation, L2: Laser–assisted bleached followed by 2Watt laser irradiation and L4: Laser–assisted bleached followed by 4Watt laser irradiation. Surface roughness was assessed three times for all the specimens: before bleaching, 24 hours after bleaching and finally 24 hours after post bleaching diode laser irradiation by utilizing profilometer. Paired samples t–test and independent samples t– test was utilized for statistical analysis at p≤0.05. Results: Both bleached groups exhibited a significant increase in the surface roughness of enamel with no statistically significant difference between them. Post bleaching diode laser irradiation at 4Watt resulted in a significant increase in surface roughness of enamel, while 2Watt diode laser irradiation resulted in non–significant increase in surface roughness of enamel. Conclusions: In–office bleaching techniques had a negative impact on enamel in terms of surface roughness. Post bleaching diode laser irradiation at 2Watt power parameter is more preferred than 4Watt power parameter.

BackgroundThe purpose of this in vitro study was to investigate the effects of water-jet flossing on the color stability and surface roughness of five resin-based composites. Material and MethodsFive commercially available composite resins were studied. Nine disc-shaped specimens (6x2mm) were fabricated from each composite. The specimens were randomly allocated into three groups and three different treatments were performed on each group: storage in water (control group), water-jet flossing using 50 Psi water pressure, and water-jet flossing using 100 Psi water pressure. The water-jet flossing was performed in a standardized manner using a Waterpik® Aquarius® water flosser. Color and roughness were measured at baseline and at the end of 30 minutes of treatment, which is approximately equivalent to 5 years of simulated water-jet flossing for 1 minute once a day. The data were statistically analyzed using two-way analysis of variance (ANOVA) with Bonferroni and Tukey’s post-hoc tests. ResultsNo significant color change was found after 5 simulated years of water-jet flossing, irrespective of composite type and water-flossing pressure setting (p > 0.05). Furthermore, none of composite specimens showed any significant surface roughness changes except for the two composites with spherical filler specimens in the 100 Psi treatment group. These composites exhibited a significant increase in surface roughness compared with the nano-filled composite (p = 0.001 and p = 0.006). However, the differences were clinically acceptable (≈0.2 µm). Conclusions In terms of surface roughness and color, water-jet flossing is safe to be used on composite restorations within the settings of this study. Key words:Color difference (∆E), resin composites, surface roughness, water flosser.

Influence of bottled salad dressings on the development of enamel erosion in the presence or absence of salivary pellicle – An in vitro study

Aims: The aims of this study were to evaluate the in vitro effect of a cocoa bean husk extract (CBHE) mouthwash in comparison with that of a fluoridated mouthwash on surface roughness of the enamel surface after subjecting the teeth to two types of energy drink challenge. Materials and Methods: Eighty (80) sound maxillary first premolar were collected and randomly divided into four groups, the teeth in the first and second groups were immersed in a tiger energy drink for 14 days and then one group in a CBHE and another in a fluoride mouth rinses for 7 days. While the remaining teeth in the third and fourth groups were immersed in a red bull energy drink for 14 days and then one group in a CBHE and another in a fluoride mouth rinses for 7 days. Enamel surface was assessed by a profilometer device at a baseline, after erosive challenge and after remineralization with the different treatment materials. Results: In all groups, there was a high statistically significant increase in surface roughness after erosive challenge. Meanwhile, there was a high statistically significant decrease in surface roughness in all groups after remineralization, with no significant differences between energy drinks or remineralization materials. Conclusion: Within the limits of the current study, cocoa bean husk extract and fluoride mouth rinses had an effective remineralizing ability after erosive energy drinks which have a destructive effect on tooth enamel. CBHE mouth wash showed a similar remineralization effect to fluoride groups.

Effect of simulated toothbrushing on the surface roughness of LOCATOR abutments: An in vitro study

Background: Alterations in the microhardness and roughness are commonly used to analyze the possible negative effects of bleaching products on restorative materials. This in vitro study evaluated the effect of in-office bleaching (SDI pola office +) on the surface roughness and micro-hardness of four newly developed composite materials (Z350XT –nano-filled, Z250XT-nano-hybrid, Z250-mico-hybrid and Silorane-silorane based). Materials and methods: Eighty circular samples with A3 shading were prepared by using Teflon mold 2mm thickness and 10mm in diameter. 20 samples for each material, 10 samples for base line measurement (surface roughness by using portable profillometer, and micro-hardness by usingDigital Micro Vickers Hardness Tester), and 10 samples for after bleaching measurement. The appropriate bleaching procedure was performed on the top surface of test groups for 90 minutes total bleaching period. Then surface roughness and hardness were tested at the end of the duration. Statistical analysis was carried out using ANOVA, LSD and t-test. Results: There was a highly significant increase in surface roughness of all tested groups after bleaching. There is a highly significant increase in micro-hardness for Z250, there is decrease in Micro-hardness for siloraneand Z250xt and there is a non-significant increase in micro-hardness of Z350xt. Conclusion: bleaching has a negative effect on surface roughness of all the tested materials, as surface roughness increased after bleaching. Micro-hardness is a material dependent, there is different reaction to bleaching depending on the resin, load and size of the fillers used in the materials. Nano-filled composite is the material that has better performance than the other tested materials, as it is the material that has the least affection by bleaching.

Aim:Comparative evaluation of commonly consumed catechu and catechu with lime on surface roughness and color stability of the conventional nano-hybrid composite.Methodology:A total of 50 uniform cylindrical disks of 10-mm diameter and 2-mm thickness prepared from the nano-hybrid composite were used in the study. Each sample was randomly divided into three subgroups of 20 samples each in two experimental groups (catechu, catechu, and lime) and 10 samples in the control group (artificial saliva). The samples were immersed in each agent for 15 days. Surface roughness and color changes measurements were noted at the baseline and 15th day by two-dimensional profilometer and spectrophotometer, respectively.Results:It was found that nano-hybrid composite resin showed more surface roughness and color change when immersed in catechu and catechu with lime as compared to the control group. Intergroup comparison showed statistical significant increase in surface roughness and color change in the catechu group followed by the catechu with the lime group and artificial saliva.Conclusion:Within the limits of the present study, it can be concluded that all experimental specimens showed discoloration. At the end of 15th day, among the groups, catechu showed more surface roughness and color change followed by the catechu and lime and the control group.