Abstract
Thermal decomposition of K 2SiF 6 is a complicated process depending on several parameters, the combination of which cause difficulty in comparing the results obtained from different methods. An experimental method for the study of small quantities of material is described. This allows direct comparison with thermoanalytical results. The influence of experimental conditions is discussed. The decomposition of K 2SiF 6 is a model for other complexes which produce easily hydrolysed products during thermal reaction. The course of thermal decomposition of K 2SiF 6 is described up to complete vaporisation of the products at 1200°C.
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