Abstract
Pentacarbonyl acyl molybdates 1 react with boron trifluoride to give difluoroboroxy Fischer carbene complexes 2, which undergo loss of the metal fragment at room temperature leading to 1,2-diketones 3, 1,2-hydroxyketones 4, or dimers 5 via a dimerization process of acyl radicals. Decomposition of 2 in the presence of 3-buten-2-one 6 furnishes the adducts 7.
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