Abstract

Abstract This paper describes the development of an instrumented and automated single mode microwave cavity for sintering ceramic powders. This setup includes an optical dilatometer and a motorized plunger to control heating cycles in a wide range of heating rates (from 5 °C ∙ min− 1 to 200 °C ∙ min− 1) up to 1600 °C and to allow reliable comparison with conventional sintering. The cavity and the sintering cells for both hybrid and direct microwave sintering were designed using finite element simulation. For accurate temperature measurement, an optical pyrometer calibrated with a specific protocol has been used. Microwave sintering of fine grained (

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