Abstract

The use of electrothermal vaporization devices (ETV) to introduce analytes into inductively coupled plasma (ICP) for determination by atomic emission spectroscopy (AES) provides detection limits in picograms but requires solution concentrations higher than nanogram‐per‐litre levels. Determination of metal concentrations lower than nanograms per litre requires a preconcentration step. The method of controlled potential electrodeposition of metals into mercury film on glassy carbon electrodes for ETV‐ICP‐AES is described. The method can be used for simultaneous multielemental determination of trace and ultratrace concentrations of metals in water. Modification and optimization of the technique are discussed. Also included are the results of determinations of eight trace elements.

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.