Abstract
Traces of manganese in uranium and its compounds can be determined by ion-exchange separation and square-wave polarography. When a 9 M hydrochloric acid solution of the sample is introduced into a column of strongly basic anion-exchange resin, manganese can be quantitatively separated from uranium by cluting with 9 M hydrochloric acid. The determination of the separated manganese by square-wave polarography is performed in 1 M potassium hydroxide-0.4 M triethanolamine solution with an excellent sensitivity. The lower limit of the method is 0.5 p.p.m. of manganese.
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