Abstract
A combined method for macroconcentrations of platinum determination in chloroplatinic acid and industrial concentrate obtained during processing of some types of electronic engineering scrap that is based on a combination of gravimetric precipitation of platinum by ammonium chloride with subsequent determination of a residual concentration of platinum in a filtrate using the ISP-AES method is developed. The errors at each stage of analysis, as well as the total error, are estimated. It is shown that the accuracy of macro-concentrations of platinum determination using the combined method is not inferior to the accuracy of classical gravimetric analysis (the relative standard deviation does not exceed 0.15% for 15–40% wt concentrations of platinum). The combined method of analysis based on a combination of gravimetry and ISP-AES makes it possible to decrease labor expenditures and the time of analysis as compared to the classical one.
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