Design and characterization of a compact Einzel lens for portable quadrupole mass spectrometry (QMS)

Abstract

Quadrupole mass spectrometry (QMS) offers better resolution, selectivity and sensitivity than the metal-oxide, field effect transistors and thermal-based gas sensors. However, existing QMS systems are unsuitable for field applications. The miniaturized QMS requires dimensionally scaled components with comparable performance to the conventional bulky systems. For a portable quadrupole mass spectrometry, a compact focusing ion system is required to transfer the maximum number of ions from the ion source to the filter. The present paper discusses the design of a miniature focusing Einzel lens and the effect of design parameters on its performance. The three-cylindrical axially symmetric compact Einzel lens assembly was designed using commercially available software. The relationship between the design parameters is explored for compact and low-powered ion optics. The beam focal length was tuned by varying the bias voltage. The dimensions, as well as voltages across the Einzel lens, were reduced significantly to open a new way for portable point-of-care applications. At an applied voltage of 70 V, the focal length of the ions is 11 mm without being scattered, which is favorable for a portable quadrupole mass filter. The designed Einzel lens was fabricated using micromachining techniques and characterized at a vacuum of 3.05 × 10−4 mbar. The developed lens system shows a current output of 0.114 µA at 72 V lens voltage. A current of 94.8 µA is observed with a background noise of 0.01 µA for the system with nitrogen (28 amu) as the sample.