Abstract
Mixed single crystals of [Co(OCN2H4)5(H2O)][ZnCl4] were grown by the isothermal evaporation of an aqueous solution. The crystal structure of this complex was established by X-ray diffraction (R = 0.052 based on 7003 reflections). The crystals consist of [Co(OCN2H4)5(H2O)]2+ cations containing Co atoms in an octahedral coordination and [ZnCl4]2−] anions containing Zn atoms in a tetrahedral coordination. The carbamide molecules are involved in both intramolecular and interionic hydrogen bonds. The H2O molecule forms hydrogen bonds with the anions.
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