Abstract
In the title compound, C7H13NOS2, the thiomorpholine ring adopts a chair conformation and the bond-angle sum at the N atom is 360°. The dihedral angle between the amide group and the thiomorpholine ring (all atoms) is 36.48 (12)°. In the crystal, C—H⋯O and C—H⋯S hydrogen bonds link adjacent molecules, forming two-dimensional networks extending parellel to the (011) plane.
Highlights
Supporting information for this paper is available from the IUCr electronic archives (Reference: HB7480)
Symmetry codes: (i) x, −y+3/2, z+1/2; (ii) x, y+1, z; (iii) x, y−1, z
Summary
C7H13NOS2, the thiomorpholine ring adopts a chair conformation and the bond-angle sum at the N atom is 360. The dihedral angle between the amide group and the thiomorpholine ring (all atoms) is 36.48 (12). C—H O and C—H S hydrogen bonds link adjacent molecules, forming two-dimensional networks extending parellel to the (011) plane. Symmetry codes: (i) x; y þ 32; z þ 12; (ii) x; y þ 1; z; (iii) x; y 1; z. Data collection: APEX2 (Bruker, 2013); cell refinement: SAINT (Bruker, 2013); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL2013 (Sheldrick, 2015); molecular graphics: DIAMOND (Brandenburg, 2010); software used to prepare material for publication: SHELXTL (Sheldrick, 2008)
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