Abstract
Crystals of 1-amino 2-phenyl benzocycloheptanol hydrobromide monohydrate are orthorhombic witha=6·927(17),b=30·947(40),c=30·990(40) A,z=16 and the space group is Iba2.ρ=1·41 gm/ccρ cal=1·403 gm/cc,μ for CuKα=37.06 cm−1. The structure was solved by heavy atom method using three dimensional x-ray intensity data and refined by block diagonal and full matrix least squares method to anR-index of 0·106. The structure is stabilised by a number of hydrogen bonds of the type N-H…O, O-H…Br, N-H…Br. The heptane rings in this molecule are in chair conformation.
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