Abstract
AbstractA convenient protocol for the synthesis of pseudopeptides containing selenomethylene [ψ(CH2Se)] moiety as amide bond surrogate is delineated, starting from Nβ‐protected amino diselenides. The key step of the synthesis stands in situ generation of selenol from diselenide, which is trapped by bromide, importantly β‐bromides. Overall, the chemistry reported here is simple.
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