Abstract

A composite gasket was designed for diamond-anvil cells where the load was supported mainly by the inner part made of NiCrAl with a diameter slightly larger than the culet of the anvil. A BeCu girdle encased the NiCrAl washer and prevented it from fracturing. The thickness of the gasket was about 30μm at a pressure of 30GPa applied with a pair of diamond anvils having 500 and 550μm culets. The magnetic contribution of the composite gasket to the background signal was almost the same as that of a BeCu gasket having the same size. The diamond anvils were fixed to the pistons with four miniature screws through small BeCu rings that were press fitted to the circumference of the diamond anvils. The performance of this composite gasket together with the anvil retainer was illustrated by the measurements of the temperature dependence of the dc magnetic susceptibility of Cs2CuF4 under various pressures up to 26GPa using a superconducting quantum interference device vibrating coil magnetometer.

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