Abstract

A complete (1)H, (19)F, and (13)C NMR assignment of a homologous series of polyfluorinated acids and alcohols is reported. These assignments were obtained chiefly through single and multiple-bond (1)H-(13)C and (19)F-(13)C correlation experiments (HSQC, HMBC). (19)F NOESY experiments were required for assignment of two compounds with diastereotopic (19)F nuclei in the CF(2)chain of the molecule.

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