Abstract

AbstractThe complete assignments of 1H and 13C data for two steroid epoxides, 3β‐acetoxy‐5,6β‐epoxyandrostan‐17‐one and 3β‐acetoxy‐5,6β‐epoxycholestane, based on DEPT, 1H1H DQF COSY, HMQC, 1D TOCSY and 2D HMQC TOCSY sequences are described. Especially the 1D TOCSY and 2D HMQC TOCSY techniques were essential to the structure elucidation of theses steroids.

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