Abstract
AbstractAdding a thermolysis step to electrosynthesis (as in “electrothermosynthesis”) considerably enhances the scope of electrochemical film deposition and affords multinary compositions previously inaccessible by this otherwise versatile and mild synthetic approach. Copper pyrovanadate (β−Cu2V2O7), a member of the Cu−V−O family of ternary oxide semiconductors that are of considerable interest to the solar fuel community, is shown herein to be an exemplar of this approach. Finally, the generality of the hybrid approach is discussed for a variety of ternary metal oxides.
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