Abstract
AbstractChromatographic reactors integrate chemical reaction and chromatographic separation in one apparatus. This offers potential for process intensification, especially in the case of equilibrium reactions. Different types of discontinuous and continuous processes as well as modeling of chromatographic reactors are described. Synthesis and design of this processes is very much influenced and often restricted by the type of reaction and the operating window which is set by the individual operating conditions for chemical reaction, mass separation, and equipment design. Integrated chromatographic reactors should be considered if chromatography is the favored separation process for a conventional sequential process design. Preparative chromatographic reactors are known for liquid‐ and gas‐phase processes. Laboratory‐scale applications are described. Analytical chromatographic reactors are used to determine reaction rate constants and kinetics, and to screen chromatographic systems and operating conditions for preparative applications.1.Introduction2.Types of Chromatographic Reactors3.Modeling of Chromatographic Reactors3.1.Adsorption Isotherm and Reaction Kinetics3.2.Modeling the BCR3.3.Modeling Simulated Moving Bed Chromatographic Reactors3.4.Process control4.Synthesis of Preparative Chromatographic Reactors4.1.Process Principles4.2.Type of Reaction5.Design of Preparative Chromatographic Reactors5.1.Design of the Process5.2.Choice of Operating Conditions6.Preparative Chromatographic Reactors6.1.Applications of Gas Chromatographic Reactors6.2.Application of Liquid Chromatographic Reactors7.Analytical Chromatographic Reactors7.1.Determination of Rate Constants7.2.Enzymatic Reactions7.3.Characterization of the Stationary Phase7.4.Examination of Fast Equilibrium Reactions7.5.Examination of Solvent Effects
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