Abstract
AbstractFour diastereomeric molecular cages based on cyclotriveratrylene (CTV) and sucrose scaffolds, connected via p‐phenylene linkers, were synthesized in a few steps synthesis. The absolute configuration of these diastereoisomers was determined by advanced NMR and ECD spectroscopies supported by DFT calculations. The X‐Ray crystal structure of P‐4 b cage gave an insight into its unique structure. The binding properties of P‐4 a and M‐4 a cages towards small ammonium guests (1‐methylpyridinium and 1,3‐dimethylimidazolium salts) were investigated.
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