Abstract
[1.1]Ferrocenylruthenocenophane was prepared by the reduction of [1.1]ferrocenylruthenocenophane-1,12-dione. [1.1]Ferrocenylruthenocenophane and [1.1]ferrocenylruthenocenophane-1,12-dione react with BF3–Et2O containing benzoquinone and give black monocationic salts analyzed as [1.1]ferrocenylruthenocenophanium+BF4− and [1 .1]ferrocenylruthenocenophane-1,12-dionium+BF4−, respectively. 57Fe-Moessbauer spectroscopic studies of the salts suggest the presence of an intramolecular electron transfer between the Ru and Fe atoms.
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