Abstract
Cyclic voltammetry in aqueous electrolyte of uranium oxides (α-U 3 O 8 , α-UO 3 , and γ-UO 3 ) mechanically transferred to a graphite electrode enables the reduction of these solids to be studied over a wide time domain. The results support a mechanism of a U(VI) to U(V) electron transfer coupled to cation diffusion to form a topochemical insertion compound at the solid electrode-electrolyte interface
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