Abstract
A series of Fe-P-B ultrafine amorphous alloy particles has been prepared by the chemical reduction method. The composition and size of the particles have been effectively adjusted. Mossbauer spectroscopy in addition to some other techniques has been used to investigate the reaction process, the factors that influence the preparation, the crystallization of the particles, and the interactions between the components within them. The results indicate that the co-deposition of iron, phosphorus and boron atoms in the solution at room temperature forms Fe-P-B amorphous alloy particles, and a preferential bonding of Fe-P bond to Fe-B one exists in the particles.
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