Abstract
Abstract The multi-selenium donor ligand 2,2-dicyanoethylene-1,1-diselenolate (DCNSe) has been prepared. The dianionic complex of DCNSe with Ni(II) has been isolated as the tetrabutylammonium (TBA) salt. The compound is characterized by negative ion Fast Atom Bombardment (FAB) mass spectral analysis, Fourier Transform Infrared (FT-IR) spectral analysis, UV-Vis spectral analysis and cyclic voltammetry. The electrochemical properties and crystal structure are studied as well. In addition, the corresponding Cu(II) complex has been isolated as the TBA salt and characterized by negative ion FAB mass spectral analysis and FT-IR spectral analysis.
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