Abstract
The paper describes the synthesis of the N-Boc lactam 4 and demonstrates that it is an important intermediate in the synthesis of dipeptide 5 (X = H, n = 0, R = Me), an analogue of the ADDA-Glu dipeptide 3. In addition we have described a mild method for the preparation of the amino acid salt ADDA·HCl and provided synthetic methods and full characterisation for the previously `elusive' free amino acid ADDA.
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Schedule a callMore From: Journal of the Chemical Society, Perkin Transactions 1
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