Abstract
-- Electrochemical treatment of caprolactam solutions in an alkaline medium on carbon electrodes reduces the permanganate number, which is connected with the appearance of amino groups, predominantly in the anolyte. The process of electroreduction is limited by concentration polarization. -- In acid medium, oxidation products are not observed, and electrochemical treatment of the regenerated lactam is fundamentally possible. -- Results from treatment of the lactam depend to a considerable degree on the nature of the electrodes and background, on the pH of the medium in the anolyte and catholyte, and on temperature.
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