Abstract
Trimethylantimony(v) diacylates Me3Sb(OCOR)2 (R = H, Me, Ph) have been obtained in 72–75 % yield by the interaction of trimethylantimony withtert-butylhydroperoxide and carboxylic acids at the ratio of 1 ∶ 1 ∶ 2 in benzene (20 °C, 20 h) in the presence of sodium sulfate.
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