Abstract

A series of 3‐phosphoryl‐2,3‐dihydrofurans are efficiently synthesized by the reaction of diethyl 1‐diazo‐2‐oxo‐alkylphosphonates with alkyl vinyl ethers in good yields. 2,3‐Dihydrofurans bearing phosphoryl and trifluoromethyl moieties are also prepared in a similar manner. #Studies on Organophosphorus Compounds, Part 132. For Part 131, see D. Gong, L. Zhang and C. Yuan, Synthetic Commun. 2004, 34 (18).

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