Abstract
The title compound, [Re(C 18 H 15 NP) 2 (C 2 H 5 O)O], was synthesized by the oxidation-substitution reaction of [Re III (PNH) 2 (PNH 2 )]Cl, where PNH 2 is 2-(diphenylphosphino)phenylamine, with NEt 3 in EtOH. The X-ray diffraction study of this new triclinic phase, designated β, confirms the molecular structural details for the monoclinic α isomer, which crystallized in space group P2 1 /c with a=12.056 (3), b=26.303 (6), c=11.005 (3) A, β=102.32 (2) o [Refosco, Tisato, Bandoli, Bolzati, Dolmella, Moresco & Nicolini (1993). J. Chem. Soc. Dalton Trans. pp. 605-618]
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