Abstract
The Ni(4) inverse metallacrown (NHEt(3)) [Ni(4)(bmo)4(Hael)2(ael)2](ClO(4))3 [(NHEt(3)).1.(ClO(4))3], with the inverse 12-MC-4 motif, has been assembled via simultaneous chelation and bridging of butan-2,3-dionemonoxime (Hbmo) and 2-amino ethanol (Hael).
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