Abstract
Abstract Anhydrous tin (II) chloride and tin (II) bromide have been prepared utilizing an apparatus designed to circulate the appropriate hydrogen halide gas over molten tin. A Teflon piston with o-ring seals in a 25mm true-bore tubing and ground glass check valves with sapphire beads served as the gas pump. With the product subliming out of the heated zone containing the metal, a fresh tin surface was continuously exposed effecting 90% conversion of hydrogen chloride and 70% conversion of hydrogen bromide to their respective anhydrous tin (II) halides.
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