Abstract

A technique for evaluating the (steady-state) creep stress exponent (n) from indentation data has come into common use over recent years. It involves monitoring the indenter displacement history under constant load and assuming that, once its velocity has stabilized, the system is in a quasi-steady state, with Stage II creep dominating the behaviour. The stress field under the indenter, and the way in which the creep strain field is changing there, are then represented by “equivalent stress” and “equivalent strain rate” values. These are manipulated in a similar manner to that conventionally employed with (uniaxial) creep test data, allowing the stress exponent, n, to be obtained as the gradient of a plot of the logarithm of the equivalent strain rate against the logarithm of the equivalent stress. The procedure is therefore a very simple one, often carried out over relatively short timescales (of the order of 1h or less). However, concerns have been expressed about its reliability, regarding the neglect of primary creep (after a very short initial transient) and about the validity of representing the stress and strain rate via these “equivalent” values. In this paper, comprehensive experimental data (both from a conventional, uniaxial loading set-up and from instrumented indentation over a range of conditions) are presented for two materials, focusing entirely on ambient temperature testing. This is supplemented by predictions from numerical (finite element method) modelling. It is shown that the methodology is fundamentally flawed, commonly giving unreliable (and often very high) values for n. The reasons for this are outlined in some detail. An attempt is made to identify measures that might improve the reliability of the procedure, although it is concluded that there is no simple analysis of this type that can be recommended.

Highlights

  • While the Young’s modulus can readily be measured via instrumented indentation, obtaining plasticity parameters from indentation data is slightly more complex

  • The following conclusions can be drawn from this work, which is focused on a commonly used methodology for obtaining creep stress exponent (n) values from indentation data – using experimental measurements of the indenter velocity, which often exhibits a tendency to stabilize quite quickly

  • (a) It has been shown, by applying the methodology to creep indentation tests carried out with almost 50 different sets of conditions, that the derived values of n exhibit a huge degree of scatter

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Summary

Introduction

While the Young’s modulus can readily be measured via instrumented indentation, obtaining plasticity parameters from indentation data is slightly more complex. A common concern during creep testing is that the specimen microstructure (grain structure, dislocation density, precipitate dispersion etc.), which can significantly affect creep behaviour, may evolve in some way during the period of the test, possibly as a consequence of high plastic strains in the immediate vicinity of the indenter. If this were a potential explanation for discrepancies between indentation-derived and conventionally obtained creep parameters, it might be expected that they would not arise with (metallic) glass samples (in which no microstructural evolution is expected to occur, assuming that there is no crystallization). Eq (1) is essentially an empirical relationship, it is sometimes possible to rationalize the observed values of n and Q in terms of some model for the rate-determining process taking place within the microstructure of the material

Indentation creep testing
Materials
Compression testing
Meshing and mechanical boundary conditions
Creep dwell curves for copper
Creep dwell curves for tin
Primary creep
Equivalent stress
Equivalent strain rate
Combined effects
Findings
Conclusions
Full Text
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