Abstract

The X-ray crystallographic study of the title compound, C37H41N3O6, at 150 K establishes the N-oxide form of the triazene 1-oxide unit. There is one intra­molecular N—H⋯O hydrogen-bonding inter­action and the crystal packing is stabilized by one N—H⋯O, three C—H⋯O and three C—H⋯π inter­molecular inter­actions. The dihedral angles between pairs of adjacent benzene rings are 14.9 (3), 56.3 (1) and 56.0 (1)°

Highlights

  • The X-ray crystallographic study of the title compound, C37H41N3O6, at 150 K establishes the N-oxide form of the triazene 1-oxide unit

  • Dimerization of two molecules (I)through intermolecular N–H···O and C–H···O hydrogen bonding interactions shown by dotted lines (Symmetry code: (i) -x + 1, -y, -z + 2)

  • Symmetry codes: (i) −x+1, −y, −z+2; (ii) x+1, y, z; (iii) x−1, y, z; (iv) x−1, y+1, z; (v) x, y−1, z

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Summary

Pradip Kumar Mandalc and Pinaki Bandyopadhyaya*

The dihedral angles between pairs of adjacent benzene rings are 14.9 (3), 56.3 (1)

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